Firebrick check mark is accurate
The product checks and accept the economic interest of the stand or fall that matters to project quality directly as a result and both sides of supply and demand. Current, of goods of our country figuration check and accept sampling standard to be GB/T10325—2012 " refractory products checks and accept boarding sampling inspection is regular " , boarding goods is aimed at on international check and accept sampling standard to be ISO5022:1979 " Shaped Refractory Products—Sampling And Acceptance Testing " . The main distinction of both depends on the size of sample size and judgement regulation: ISO 5022 is based on statistical principle to use large sample size, the inhomogenous sex of mature fireproof material and production and use square profit impact, more major and reasonable.
One, fireproof material arrange turns performance detect:
1, of firebrick detect project: Temperature of bate of stability of intensity of compression of content of main and chemical component, normal temperature, thermal shock, loading 4 projects.
2, fireproof and pouring of makings detect project: Intensity of content of main and chemical component, compression, fight fold density of ratio of change of the intensity, line after burning, bulk 5 projects. Afore-mentioned manage turn performance detect should check a center to detect to the fireproof material product quality supervision and inspection of national attestation.
2, firebrick convention detects record and watch of circumstance of processing exceeding bid
The composition of 1. firebrick fills in.
2. why the error of big head, small head allows 1mm, length error allows 2mm, high error allows 1% . Explanation: 1mm of error of big, small head can adjust with plaster, length error 2mm can expand through bricky lateral chipboard and plaster will adjust. Height allows 1% , this is one kind represents a form, the firebrick that uses inside group kiln has 3 kinds of different height: 200mm, 220mm, 250mm. The error limitation of different height brick is different, but cannot exceed 2-2.5mm, usually, we should be controlled in 1-1.5mm. Also fireclay can adjust this error.
3. flatness: Control is in 0.5mm. Explanation: The feet that use stuff will detect the level level of bricky bedding face, norms of commonly used feet of a place of strategic importance has 0.1, 0.2, 0.25, 0.3, 0.4, 6 kinds 0.5. The flatness maximum of firebrick cannot exceed 0.5mm. On the operation, we had better be control is in 0.2-0.3mm is advisable. Can adopt the rule of a place of strategic importance of 0.5mm, the flatness that shows this brick is bad, should many a few box, measure a few more (because exceed the mark fiducial value of 0.5mm,this is, when heal, the brick crushs easily; As a result of,the brick is in inside kiln after production the roll of kiln, bricky bedding face squashs each other, disintegrate of easy also generation) if still be such word, answer to be contacted with the supplier, by owner, we, the supplier decides corresponding construction build by laying bricks or stones to build program jointly. And by supplier acceptance this approves bricky service mass.
Does 4. sheet weigh: ? Dash forward tip of Mie of ブ of Zhang of Hu ┑ Mu Li attacks about be contrary to neon of ┑ of of wall of cheek of N of copy of ┑ of Mao of aunt of Ъ of miscellaneous trade of ministry tip guides Qi Kan Ran of big pool of whetstone of Rong of hand Qi thirsty cowardly hopes Bo dash forward Hu ┑ takes Du to take = dainty. If lay particular stress on explains firebrick dimension may slant big, or be affected with damp be affected with damp; Slant light specification porosity density of standard of pine of big, quality of a material, short of. To exceeding the brick of limits, the supplier does not have specification and acceptance, need not use.
Mark of 5. edge caustic, horn caustic, crackle, indentation, frit, beat includes an explanation: These blemish are firebrick is in make, firing, pack, the carriage process injury in generation and blemish, afore-mentioned phenomena should be only inside the scale on form, it is the brick that can use. Will tell commonly, sample 6 bricks are not due these cases appear, if discovery has one to go to 2, should reopen one box, still have this kind of appearance, should contact a supplier, inquiry circumstance. Had done relevant equipment to forget.
3, firebrick quality certificate:
1, keep a book character
2, leave factory product theory index and experiment method
3, construction instructor
4, brick graph
5, product container load plan
6, product certificate of approval
These are acceptable according to.
4, firebrick sampling is regular: Firebrick norms and dimension, exterior, section checks the sample that examines with academic performance, use random sampling method: Every approve exterior quality with 10 tons of in the limit of, manage turns performance every batches undertake sampling with 60 tons of in the limit of. The exterior, dimension, sheet examines again take 20, manage changes function to examine take 6. Amount of sampling of firebrick of every kinds of model is not gotten little at 3.
The product checks and accept need to pay close attention to 3 respects: The validity that the representative, method of sampling chooses, detect the accuracy of the result.
One, Of sampling representative
Use normally detect of sample detect the result will decide a batch of material are received. Be those who assure a sample thief is representative, before sampling, the amount of the sort that the related side should inspect data, contract, delivery, Chu Yunfang that pack type those who wait is different, the sampling inspection plan that adopts is reached consistent. According to GB/T10325—2012, a detailed, effective sampling inspection program should include:
(1) group by group or group approve methodological;
(2) sampling method and program;
(3) checks the several; of the project
(4) examines in the light of every the technical requirement; that project place uses experiment method
(Every sample that 5) place chooses whether use at many purposes to detect;
(Quantity of 6) sampling requirement, sampling, quality is characteristic an experiment method and the quantitative; that check sample
(7) basis sample detects the regular; that approves product quality to undertake assess to examining as a result
(8) if generator and user have a difference of opinions as a result to examining, solve; of this divergent way
(9) sampling plan writes down those who reach its to carry out to supervise really should be assumed by the expert that be familiar with shaddock model problem not only and dawns very familiar production and goods are used.
Should notice, not be all quality character that offers in product quality standard or technical requirement must serve as check and accept examine project. According to ISO5022, refractory to boarding products, should choose chemical composition and the main physics character that do not exceed 3 opposite independence to regard as check and accept examine project.
In sampling, make appearance, sample deliver, store in the process, want to notice not to change the test performance of material savagery, prevent to wait for measure property to produce any changes. For example magnesian calcic brick must sealed, delivering, store avoid to suck tide in the process.
Need is special those who point out is sampling amount problem, GB/T10325—2012 and photograph of GB/T10325—2001 of on one edition compare big modification than having, will original 100~300t is ≤500t is a batch to be adjusted one batch, introduced the idea of several manage statistic, but sample size still is less than international standard ISO5022. Is what basically use when is the product checked and accept at present GB/T10325—2001: ? ? example, unqualified when times doubler answer check, simple only cost decides. Actually, ISO5022 uses large sample size, the method that uses several manage count completely undertakes judging as a result to detecting, the requirement is whole batch the uniformity of product quality, considered the venture with joint both sides of supply and demand. Taste the even, stability of quality to assure to produce, should say ISO5022 is more scientific, reasonable, the hope uses ISO5022 extensively in fireproof material production and use link as soon as possible.
2, method and the validity that the condition chooses
When material detects, chooses experiment method and experiment condition want with detect material and the standard that technical contract place asks are uniform. For example, to index of loading bate temperature, the standard that at present home implements has " method of experiment of temperature of bate of loading of GB/T5989—2008 fireproof material shows difference to warm up law " and " YB/T370—2016 is fireproof method of experiment of temperature of material loading bate (blame show difference - warm up law) " . Be aimed at same a product, of both detect the difference that has 50 ℃ left and right sides as a result. Use different method to matter to a result directly eligible. Be aimed at compact figuration goods and goods of boarding heat insolation, experiment condition also has a difference. It is with loading bate temperature likewise exemple, the loading of compact figuration goods is 0.2MPa, and loading of goods of boarding heat insolation is 0.1MPa or 0.05MPa. Different loading is affected directly detect result.
3, detect the accuracy of the result
In routine, often can discover different lab between detect data has difference, bring about the person that use not to know to which should believe - detect data. To an eligible lab, due and severe quality control measure will assure to detect the accuracy of the result. Basis " the current requirement that GB/T27025—2008 detects and calibration experiment slaughters ability " , normally detect quality control method has the following kinds:
(1) uses reference materials or reference standard undertakes in-house quality controls;
(2) attends compare between the lab right or ability test and verify plans;
(3) uses identical or different methodological retest;
(4) detects again to withholding sample to undertake;
(5) tastes the dependency of different and characteristic result to analyse like some.
To detecting through designedly mobile process and result carry out quality to control, come test and verify and evaluation detect mobile effectiveness and the accuracy that check a result, assure to detect thereby the quality of the result.
In the meantime, sample preparation serves as one of detected processes, also should undertake controlling, avoid to control appearance process to detecting the effectiveness of the result produces an effect.
If choose tripartite lab to undertake examining checking and accept, should choose to have the lab of aptitude. The job that the lab chooses to abide by criterion:
(1) chooses the laboratory of governmental authorization, identify inspect for example appoint the market station of accredit of the national center of accredit, local government or; of qualitative check courtyard
(2) obtains Chinese lab to approbate the lab that committee approbates. The place on put together is narrated, before refractory products is checked and accept, the character that answers a product has a sufficient knowledge, according to its character is mixed check and accept a project to make detailed sampling plan, determine detected method. If choose tripartite lab to undertake examining, still should undertake choosing to the lab, ensure check and accept reasonable and effective.
One, sampling standard
1) sampling is regular: According to every batches battlements number, platoon is counted and the real passion of the exterior wishs sampling, wu begs interval even, take care of comprehensive. Sampling should press firebrick date group by group, if the amount is too little, can incorporate by several bricks date a batch (should be) of same work number, in several bricks date, choose date of representative a kind of brick serves as sample.
Appearance and dimension are checked. When taking 10, can have 1, when taking 20, the numerical value that can two do not taste a regulation under below one class (seconds forbids to set numeric) under the standard. Be like unqualified when, should search a pile new sampling answer check.
The examination of section: Every batches of appearances selective examination 20 when, among them 6 examinations section, the numerical value that can 1 tastes a regulation under below one class (seconds forbids to set under the standard) ; appearance selectives examination 10 when, among them 3 examinations section, should all qualification. Be like unqualified when, should search a pile new sampling answer check.
2) sampling amount: Approve bulk according to bricky sort, breed, norms and brick, , sampling amount pursues as follows.
2, law of firebrick check proved recipe
The appearance of fireproof material, dimension, norms, substandard that pack watchs quality, usable eye view, feel or have the aid of undertake examining at measuring a tool. Quality index, the method that uses physical function test or chemical analysis undertakes examining; is fireproof those who spend determine by YB368—75, bate temperature presses YB370—75, intensity of normal temperature compression presses YB371—75, the determines to set by the standard such as YB365—75 method of Al2O3 content undertakes.
1, structural function: Density of porosity, bulk, bibulous rate, air permeability, stomatic aperture distributings, intensity of grain bulk density, apparent pore rate, true density, compression, linear expansion the; such as the shrinkage of rate, line, granuality, sex that fight broken bits
2, mechanical function: Compression intensity, tensile strength, fight lose strength, fight roll sex of intensity, shear strength, impact strength, wearability, creep, bonding strength, stretch model index of compressibility of quantity, hot condition, melt, extruding seams an experiment to wait for;
3, heat function: The; such as stability of thermal conductance, hot coefficient of expansion, specific heat, thermal capacitance, coefficient of thermal conductivity, hot emissive rate, thermal shock
4, fire prevention grade: Density of sex of fire resistance properties, ignition, noxiousness yield smoke, smoke, heat is released reach flue gas; the calorific value of fireproof function, burning behavior, combustion, function that fight fire, high temperature resistant grade of function, fire prevention checks;
5, performance characteristics: Fireproof degree, the sex of the loading bate temperature, heavy change that burn a line, heatproof shake, sex that fight broken bits, fight acidity, fight alkalescent, fight to hydrate the gender, aggressivity that fight CO, conductivity, fight oxidisability, permanent line index of stability of change, thermal shock, plasticity, chemical analysis
Fireproof material detects executive standard
GB/T 19666-2005 is flame retardant with general rule of fireproof wire cable
GB/T 23293-2009 nitride combines refractory products and its form a complete set fireproof slop
GB/T 23294-2009 wear-resisting is fireproof material
GB/T 4513.1-2015 indeterminate form is fireproof material the 1st part: Introduce and classify
GB/T 4513.2-2017 indeterminate form is fireproof material the 2nd part: Sampling
GB/T 4513.3-2017 indeterminate form is fireproof material the 3rd part: Basic and characteristic
GB/T 4513.4-2017 indeterminate form is fireproof material the 4th part: Pouring of makings fluidity determine
GB/T 4513.5-2017 indeterminate form is fireproof material the 5th part: Sample preparation and pretreatment
GB/T 4513.6-2017 indeterminate form is fireproof material the 6th part: Of physical function determine
GB/T 4513.7-2017 indeterminate form is fireproof material the 7th part: Of prefabricated component determine
GB/T 4513.8-2017 indeterminate form is fireproof material the 8th part: Of special function determine
GB/T 14983-2008 fireproof material fights basic test method
GB/T 17601-2008 fireproof data bears vitriolic erode experiment method
Wearability of normal temperature of GB/T 18301-2012 fireproof material tries proved recipe way
Chemical analysis of spectrum of fluorescence of ray of X of GB/T 21114-2007 fireproof material - founding glass piece law
GB/T 29650-2013 fireproof material fights method of experiment of carbon monoxide sex
Density of bulk of grain of GB/T 2999-2016 fireproof material tries proved recipe way
Normal temperature of GB/T 3001-2017 fireproof material is fought change pressure test method
High temperature of GB/T 3002-2017 fireproof material is fought change pressure test method
High temperature of GB/T 34217-2017 fireproof material is fought twist pressure test method
Method of pressure test of compression of high temperature of GB/T 34218-2017 fireproof material
Tensile strength of normal temperature of GB/T 34219-2017 fireproof material tries proved recipe way
Tensile strength of high temperature of GB/T 34220-2017 fireproof material tries proved recipe way
True density of GB/T 5071-2013 fireproof material tries proved recipe way
Method of pressure test of compression of normal temperature of GB/T 5072-2008 fireproof material
GB/T 5073-2005 fireproof material presses creep experiment method
GB/T 5988-2007 fireproof material heats method of experiment of permanent line change
Method of experiment of temperature of bate of loading of GB/T 5989-2008 fireproof material shows difference to warm up law
Method of experiment of coefficient of thermal conductivity of GB/T 5990-2006 fireproof material (hot line law)
Heat of GB/T 7320-2008 fireproof material expands experiment method
Heat of GB/T 7320-2018 fireproof material expands experiment method
GB/T 7322-2017 fireproof material is fireproof spend experiment method
Water content of GB/T 3007-2017 fireproof material tries proved recipe way
GB/T 8931-2007 fireproof material fights method of experiment of broken bits sex
GB/T 30873-2014 fireproof material fights method of experiment of thermal shock sex
Of the sulfur content in GB/T 34175-2017 fireproof material determine
Of the B2O3 in GB/T 32177-2015 fireproof material determine
Yang model measures trends of GB/T 30758-2014 fireproof material experiment method (swash of arteries and veins brace up law)
Yang model measures trends of high temperature of GB/T 34186-2017 fireproof material experiment method (swash of arteries and veins brace up law)
Atom of plasma of coupling of inductance of GB/T 34333-2017 fireproof material launchs spectrum (ICP-AES) analytic method
Method of experiment of coefficient of thermal conductivity of GB/T 36133-2018 fireproof material (platinic resistor thermometer law)
Chemical analysis of GB/T 32179-2015 fireproof data is wet, atomic absorb spectral law (AAS) shoot spectral way with atom of inductance coupling plasma (ICP-AES) general requirement
GB/T 32178-2015 prismatic law determines chromium of the 6 price in containing chromic fireproof material analyses a method
Upside of furnace of GB/T 32283-2015 kiln fights gas with fireproof material caustic experiment method
Kiln of GB/T 35172-2017 cement fights method of experiment of aggressivity of combustible of life rubbish pretreatment with fireproof material
GB/T 34176-2017 adjacent 2 nitrogen miscellaneous humble is prismatic photometry determines in fireproof material diatomic learn to analyse a method with tervalent iron ionization
Fireproof material antiknock cracks GB/T 36134-2018 indeterminate form sexual experiment method
GB/T 5070-2015 contains method of chemical analysis of chromic fireproof data
GB/T 4984-2007 contains zirconium method of fireproof data chemical analysis
GB/T 5069-2015 magnalium fastens method of fireproof data chemical analysis
GB/T 6900-2016 aluminous silicon fastens method of fireproof data chemical analysis
GB/T 6901-2017 silicon is qualitative method of fireproof data chemical analysis
GB/T 16555-2017 contains carbon, carborundum, nitride method of fireproof data chemical analysis